4L7F
Co-crystal Structure of JNK1 and AX13587
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-BM |
Synchrotron site | APS |
Beamline | 22-BM |
Collection date | 2010-02-17 |
Spacegroup name | H 3 |
Unit cell lengths | 135.802, 135.802, 94.208 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 1.950 |
R-factor | 0.1624 |
Rwork | 0.161 |
R-free | 0.19770 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.470 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.950 |
Number of reflections | 47064 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |