4L7F

Co-crystal Structure of JNK1 and AX13587

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-BM
Synchrotron site	APS
Beamline	22-BM
Collection date	2010-02-17
Spacegroup name	H 3
Unit cell lengths	135.802, 135.802, 94.208
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	50.000 - 1.950
R-factor	0.1624
Rwork	0.161
R-free	0.19770
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.015
RMSD bond angle	1.470
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.950
Number of reflections	47064

Crystallization Conditions

crystal ID	method	pH	temperature	details
1