4L25
Crystal structure of DNA duplex containing consecutive T-T mispairs
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 100 |
Collection date | 2011-10-16 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 27.340, 39.330, 30.680 |
Unit cell angles | 90.00, 98.28, 90.00 |
Refinement procedure
Resolution | 19.080 - 1.100 |
Rwork | 0.231 |
R-free | 0.24050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4l26 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.895 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | PHENIX |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.100 |
High resolution limit [Å] | 1.100 |
Number of reflections | 24441 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | Sodium Cacodylate, Spermine tetrahydrochloride, 2-methyl-2,4-pentanediol, ammonium chloride , pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |