4KXM
Crystal structure of DNPH1 (RCL) WITH N6-ISOPENTENYL-AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Detector technology | CCD |
Collection date | 2010-11-18 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979756 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 32.146, 96.568, 79.034 |
Unit cell angles | 90.00, 101.58, 90.00 |
Refinement procedure
Resolution | 38.710 - 2.240 |
R-factor | 0.1765 |
Rwork | 0.174 |
R-free | 0.22720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4fyi |
RMSD bond length | 0.008 |
RMSD bond angle | 1.146 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.970 | 2.390 |
High resolution limit [Å] | 2.240 | 2.240 |
Rmerge | 0.050 | 0.107 |
Number of reflections | 21068 | |
<I/σ(I)> | 11.1 | 6.7 |
Completeness [%] | 92.0 | 65.4 |
Redundancy | 3.4 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 18% PEG8K, 100 MM NaCaCo, 200 MM ZINC ACETATE, PH 6.5, vapor diffusion, hanging drop, temperature 291K |