4KVK
Crystal structure of Oryza sativa fatty acid alpha-dioxygenase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-07-23 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 72.460, 128.583, 188.740 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 106.270 - 1.980 |
R-factor | 0.16724 |
Rwork | 0.166 |
R-free | 0.19200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.050 |
Data reduction software | XDS |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 106.270 | 2.080 |
High resolution limit [Å] | 1.980 | 1.980 |
Rmerge | 0.054 | 0.516 |
Number of reflections | 61897 | |
<I/σ(I)> | 22 | 3.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.6 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.1 | 300 | 45% PEG 400, 0.2M lithium chloride, 0.1M sodium citrate, pH 6.1, VAPOR DIFFUSION, SITTING DROP, temperature 300K |