Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4KTS

Bovine trypsin in complex with microviridin J at pH 8.5

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2013-03-16
DetectorPSI PILATUS 6M
Wavelength(s)1.0
Spacegroup nameP 21 21 21
Unit cell lengths57.330, 64.490, 71.210
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution15.000 - 1.300
R-factor0.10716
Rwork0.106
R-free0.12829
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3myw
RMSD bond length0.023
RMSD bond angle2.086
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwareREFMAC (5.7.0029)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.400
High resolution limit [Å]1.3001.300
Rmerge0.0430.448
Number of reflections65291
<I/σ(I)>20.64.6
Completeness [%]99.599.6
Redundancy5.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.52930.1 M Tris, 0.2 M lithium sulfate, 25% PEG 3350 , pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K

225158

PDB entries from 2024-09-18

PDB statisticsPDBj update infoContact PDBjnumon