4JXM
Crystal structure of RRP9 WD40 repeats
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-10-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97923 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 63.746, 63.746, 167.601 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.110 - 1.920 |
R-factor | 0.1668 |
Rwork | 0.165 |
R-free | 0.20390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3psl |
RMSD bond length | 0.014 |
RMSD bond angle | 1.416 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.950 |
High resolution limit [Å] | 1.920 | 5.210 | 1.920 |
Rmerge | 0.184 | 0.071 | 0.906 |
Number of reflections | 27436 | ||
<I/σ(I)> | 4.7 | ||
Completeness [%] | 100.0 | 99.5 | 100 |
Redundancy | 15.4 | 13.5 | 14.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 291 | 25% PEG3350, 0.2 M ammonium acetate, 0.1 M HEPES sodium, pH 7.5, VAPOR DIFFUSION, temperature 291K |