4JP4
Mmp13 in complex with a reverse hydroxamate Zn-binder
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-01 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97910 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 135.616, 36.130, 95.755 |
Unit cell angles | 90.00, 131.02, 90.00 |
Refinement procedure
Resolution | 51.160 - 1.430 |
R-factor | 0.1525 |
Rwork | 0.151 |
R-free | 0.17550 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.476 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 54.000 |
High resolution limit [Å] | 1.430 |
Number of reflections | 62827 |
Completeness [%] | 95.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 292 | 27.5% PEG 4000, 1.25M AmFormate, 100mM TrisHCl pH 8.5 , VAPOR DIFFUSION, HANGING DROP, temperature 292K |