4JN1
An Antidote for Dabigatran
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Detector technology | CCD |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 113.132, 78.217, 63.434 |
| Unit cell angles | 90.00, 89.91, 90.00 |
Refinement procedure
| Resolution | 40.000 - 1.890 |
| R-factor | 0.1769 |
| Rwork | 0.176 |
| R-free | 0.19660 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.050 |
| Refinement software | BUSTER (2.11.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 39.109 |
| High resolution limit [Å] | 1.890 |
| Number of reflections | 75791 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
