4JIO
Bro1 V domain and ubiquitin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-05-04 |
Detector | NOIR-1 |
Wavelength(s) | 0.9788915 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.430, 92.320, 229.450 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.488 - 3.600 |
R-factor | 0.3716 |
Rwork | 0.366 |
R-free | 0.42110 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.665 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.490 | 3.620 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmerge | 0.084 | 0.611 |
Number of reflections | 17664 | |
<I/σ(I)> | 6.6 | 1.7 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 7.14 | 7.29 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 0.1 M bis-Tris propane pH 7, 0.2-0.4 M sodium malonate, 15-20% PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 291K |