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4J45

Crystal structure of XIAP-BIR2 domain with ATAA bound

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2012-10-21
DetectorDECTRIS PILATUS 6M
Spacegroup nameI 4 2 2
Unit cell lengths74.504, 74.504, 108.799
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution37.840 - 1.480
R-factor0.17425
Rwork0.172
R-free0.21590
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)4j3y
RMSD bond length0.016
RMSD bond angle1.689
Data reduction softwareXDS
Data scaling softwareSCALA
Refinement softwareREFMAC (5.7.0032)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]38.0001.560
High resolution limit [Å]1.4801.480
Rmerge0.0470.479
Number of reflections25875
<I/σ(I)>26.15.2
Completeness [%]99.999.9
Redundancy12.713.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP72921.7-1.9 M ammonium sulfate, 125 mM bis-tris propane, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 292K

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