4IUM
Equine arteritis virus papain-like protease 2 (PLP2) covalently bound to ubiquitin
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-06-29 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 1.28243, 1.28289, 1.27347 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.320, 62.040, 84.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.020 - 1.450 |
R-factor | 0.1612 |
Rwork | 0.160 |
R-free | 0.17810 |
Structure solution method | MAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.413 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX (1.7.1_743) |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.110 | 1.530 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.049 | 0.205 |
Number of reflections | 36344 | |
<I/σ(I)> | 7.1 | |
Completeness [%] | 99.4 | 96.2 |
Redundancy | 8.7 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 293 | 100 mM MES, pH 6.2, 18% PEG20000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |