4IRD
Structure of Polymerase-DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.690, 56.880, 110.930 |
Unit cell angles | 90.00, 93.99, 90.00 |
Refinement procedure
Resolution | 43.280 - 2.480 |
R-factor | 0.21644 |
Rwork | 0.213 |
R-free | 0.27671 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.763 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.610 |
High resolution limit [Å] | 2.480 | 2.480 |
Rmerge | 0.059 | 0.522 |
Number of reflections | 36659 | |
<I/σ(I)> | 11.3 | 2.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 3.8 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | 15% MPD , pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |