4IHO
Crystal structure of H-2Db Y159F in complex with chimeric gp100
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-09-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.93927 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 90.661, 146.011, 187.585 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.100 - 2.800 |
R-factor | 0.25222 |
Rwork | 0.249 |
R-free | 0.30541 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ch1 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.447 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.100 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 30269 | |
Completeness [%] | 100.0 | 99 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 1.6-1.8M NH4SO4, 100mM Tris HCl, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |