4HTC
THE REFINED STRUCTURE OF THE HIRUDIN-THROMBIN COMPLEX
Experimental procedure
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 90.540, 90.540, 132.040 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 7.000 - 2.300 |
| R-factor | 0.173 |
| RMSD bond length | 0.021 |
| RMSD bond angle | 0.051 |
| Refinement software | PROFFT |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 4.5 * | Rydel, T.J., (1990) Science, 249, 277 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | PEG4000 | 28-30 (%) | |
| 2 | 1 | reservoir | 0.2 (M) | ||
| 3 | 1 | reservoir | sodium acetate | 0.1 (M) | |
| 4 | 1 | reservoir | 1 (mM) |
