4HTC
THE REFINED STRUCTURE OF THE HIRUDIN-THROMBIN COMPLEX
Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 90.540, 90.540, 132.040 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.300 |
R-factor | 0.173 |
RMSD bond length | 0.021 |
RMSD bond angle | 0.051 |
Refinement software | PROFFT |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 4.5 * | Rydel, T.J., (1990) Science, 249, 277 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG4000 | 28-30 (%) | |
2 | 1 | reservoir | 0.2 (M) | ||
3 | 1 | reservoir | sodium acetate | 0.1 (M) | |
4 | 1 | reservoir | 1 (mM) |