4HK0
UCA Fab (unbound) from CH65-CH67 Lineage
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-02-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97919 |
Spacegroup name | P 62 |
Unit cell lengths | 102.004, 102.004, 163.085 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.195 - 2.497 |
R-factor | 0.2087 |
Rwork | 0.206 |
R-free | 0.25840 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.603 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.540 |
High resolution limit [Å] | 2.497 | 6.780 | 2.497 |
Rmerge | 0.078 | 0.033 | 0.365 |
Number of reflections | 33216 | ||
<I/σ(I)> | 10.4 | ||
Completeness [%] | 99.7 | 100 | 99.1 |
Redundancy | 7.2 | 7.4 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 291 | 1.6 M ammonium sulfate, 100 mM sodium acetate, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |