4HJX
Crystal structure of F2YRS complexed with F2Y
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-08-23 |
Detector | Rigaku Satun 944 HG |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 101.307, 101.307, 71.779 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.594 - 2.910 |
R-factor | 0.2135 |
Rwork | 0.211 |
R-free | 0.26760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1j1u |
RMSD bond length | 0.002 |
RMSD bond angle | 0.567 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP (- auto MR) |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.010 |
High resolution limit [Å] | 2.910 | 2.910 |
Rmerge | 0.105 | 0.448 |
Number of reflections | 16105 | |
<I/σ(I)> | 17.5 | 3.3 |
Completeness [%] | 99.7 | 99.8 |
Redundancy | 6.8 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |