4HGT
Crystal structure of ck1d with compound 13
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E DW |
| Temperature [K] | 100 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.170, 72.970, 89.330 |
| Unit cell angles | 90.00, 103.63, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.800 |
| Rwork | 0.240 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.032 | 0.154 |
| Number of reflections | 53247 | |
| Completeness [%] | 93.3 | 89.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 100 mM Citrate, 1.0 M LiCl, 30% PEG6000 , pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
