4HGT
Crystal structure of ck1d with compound 13
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E DW |
Temperature [K] | 100 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.170, 72.970, 89.330 |
Unit cell angles | 90.00, 103.63, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.800 |
Rwork | 0.240 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.032 | 0.154 |
Number of reflections | 53247 | |
Completeness [%] | 93.3 | 89.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 100 mM Citrate, 1.0 M LiCl, 30% PEG6000 , pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |