Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2011-03-09 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.485, 77.485, 36.986 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.752 - 2.300 |
R-factor | 0.1795 |
Rwork | 0.174 |
R-free | 0.23090 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.062 |
Data reduction software | AUTOMAR |
Phasing software | AutoSol |
Refinement software | PHENIX ((phenix.refine: 1.6.1_357)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.530 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 5354 | |
Completeness [%] | 99.9 | 99 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | Sodium chloride, EuCl3, sodium acetate, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K, temperature 293.0K |