4GZ2
Mus Musculus Tdp2 excluded ssDNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-01 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.483, 42.972, 107.951 |
Unit cell angles | 90.00, 95.89, 90.00 |
Refinement procedure
Resolution | 24.472 - 1.850 |
R-factor | 0.2075 |
Rwork | 0.205 |
R-free | 0.24540 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.027 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.920 |
High resolution limit [Å] | 1.850 | 3.990 | 1.850 |
Rmerge | 0.119 | 0.084 | 0.404 |
Number of reflections | 45439 | ||
<I/σ(I)> | 10 | ||
Completeness [%] | 97.4 | 97.5 | 93.6 |
Redundancy | 3.1 | 3.4 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8.5 | 293 | 22% PEG 3350, 100mM Tris, 250mM Mg(CO2)2, pH 8.5 , VAPOR DIFFUSION, temperature 293K |