4GTU
LIGAND-FREE HOMODIMERIC HUMAN GLUTATHIONE S-TRANSFERASE M4-4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 289 |
Detector technology | AREA DETECTOR |
Collection date | 1997-08 |
Detector | SIEMENS X1000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.000, 215.700, 94.560 |
Unit cell angles | 90.00, 97.40, 90.00 |
Refinement procedure
Resolution | 10.000 - 3.300 |
Rwork | 0.245 |
R-free | 0.31500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gtu |
RMSD bond length | 0.008 |
RMSD bond angle | 1.279 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.400 | 3.500 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.165 | 0.570 |
Number of reflections | 30754 | |
Completeness [%] | 76.2 | 68.4 |
Redundancy | 2.3 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 5.6 | 22% PEG4000, 0.1M NA CITRATE,0.2M AMMONIUM ACETATE, PH5.6 |