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4GTQ

FTase in complex with BMS analogue 12

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyCCD
Collection date2009-11-01
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.0000
Spacegroup nameP 61
Unit cell lengths172.397, 172.397, 69.781
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution29.910 - 2.600
R-factor0.17383
Rwork0.171
R-free0.22269
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3eu5
RMSD bond length0.017
RMSD bond angle1.603
Data reduction softwareMOSFLM
Data scaling softwareXSCALE
Phasing softwarePHASES
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]29.9102.700
High resolution limit [Å]2.6002.600
Number of reflections36611
<I/σ(I)>16.35.3
Completeness [%]99.999.9
Redundancy5.65.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.529220% (w/v) PEG 4000, 0.2M MgCl2, 0.1M Tris, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 292K

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