4GKN
A2-MHC Complex carrying FATGIGIITV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-30 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97630 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 202.444, 46.590, 116.624 |
Unit cell angles | 90.00, 121.53, 90.00 |
Refinement procedure
Resolution | 99.400 - 2.753 |
R-factor | 0.2113 |
Rwork | 0.206 |
R-free | 0.29950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3hg1 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.698 |
Data reduction software | xia2 |
Data scaling software | SCALA (3.3.15) |
Phasing software | PHASER (2.1.4) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 99.404 | 99.404 | 2.820 |
High resolution limit [Å] | 2.753 | 12.310 | 2.753 |
Rmerge | 0.060 | 0.597 | |
Total number of observations | 1086 | 6938 | |
Number of reflections | 24462 | ||
<I/σ(I)> | 6.9 | 10.1 | 1.3 |
Completeness [%] | 99.7 | 98.8 | 99.9 |
Redundancy | 3.9 | 3.5 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 25% PEG 8000, 200 mM Ammonium Sulphate, 200 mM MES Buffer, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 293K |