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4GK4

Human EphA3 Kinase domain in complex with ligand 90

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsBRUKER AXS MICROSTAR
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2011-03-27
DetectorMAR scanner 345 mm plate
Wavelength(s)1.5418
Spacegroup nameP 1 21 1
Unit cell lengths53.067, 38.182, 75.841
Unit cell angles90.00, 101.49, 90.00
Refinement procedure
Resolution30.777 - 2.100
R-factor0.1762
Rwork0.173
R-free0.22620
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2gsf
RMSD bond length0.007
RMSD bond angle1.365
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.7.1_743))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]38.1802.210
High resolution limit [Å]2.1002.100
Rmerge0.0860.334
Number of reflections17532
<I/σ(I)>10.63.9
Completeness [%]98.893.4
Redundancy3.53.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52930.1M sodium cacodylate pH 6.5, 0.15M ammonium sulf ate, 22.5% PEG 3350 , VAPOR DIFFUSION, HANGING DROP, temperature 293K

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