Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4FQZ

Crystal structure of a protease-resistant mutant form of human galectin-8

Replaces:  3NAJ
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-5A
Synchrotron sitePhoton Factory
BeamlineBL-5A
Temperature [K]100
Detector technologyCCD
Collection date2010-05-14
DetectorADSC QUANTUM 315r
Wavelength(s)1.0
Spacegroup nameP 43 21 2
Unit cell lengths79.259, 79.259, 129.820
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution37.980 - 2.800
R-factor0.209
Rwork0.209
R-free0.25300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2yv8
RMSD bond length0.008
RMSD bond angle1.500
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.900
High resolution limit [Å]2.8002.800
Rmerge0.0960.385
Number of reflections10378
<I/σ(I)>9.33.3
Completeness [%]95.692.8
Redundancy5.35.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP929310% PEG 20000, 0.1M Bicine, 2% Dioxane, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon