4FLJ
Human MetAP1 with bengamide analog Y08, in Mn form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Detector technology | CCD |
Detector | ADSC QUANTUM 210r |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.992, 77.355, 48.479 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.580 - 1.740 |
R-factor | 0.1997 |
Rwork | 0.198 |
R-free | 0.23230 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.025 |
RMSD bond angle | 2.019 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.780 |
High resolution limit [Å] | 1.740 | 4.750 | 1.750 |
Rmerge | 0.089 | 0.054 | 0.562 |
Number of reflections | 35919 | ||
<I/σ(I)> | 11.8 | ||
Completeness [%] | 99.9 | 99.2 | 99.5 |
Redundancy | 3.6 | 3.7 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | microbatch under oil | 8 | 200 mM sodium acetate, 20% PEG 3350, pH 8.0, microbatch under oil |