4FIW
X-ray crystal structure of Corynebacterium glutamicum Nrdh-redoxin at 1.5A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 61.770, 61.770, 77.190 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.675 - 1.501 |
R-factor | 0.1931 |
Rwork | 0.191 |
R-free | 0.21340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 1R74 1h75 3IC4 and 1ABA |
RMSD bond length | 0.008 |
RMSD bond angle | 1.060 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | BALBES |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.675 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 14472 | |
Completeness [%] | 98.3 | 94.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293.15 | 12% glycerol, 0.1M Tris pH 8.5, 1.8M ammonium sulphate, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K |