4FD3

Crystal structure of apo-formed ymtOAR1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2010-07-06
Detector	RAYONIX MX225HE
Wavelength(s)	0.9793
Spacegroup name	I 41 2 2
Unit cell lengths	170.832, 170.832, 316.222
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.200 - 2.600
R-factor	0.2309
Rwork	0.229
R-free	0.27404
Structure solution method	SAD
RMSD bond length	0.010
RMSD bond angle	1.303
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	REFMAC (5.5.0072)

Data quality characteristics

	Overall
Low resolution limit [Å]	48.200
High resolution limit [Å]	2.600
Number of reflections	67051
Redundancy	13.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION	6	285	3.0 M sodium chloride, 0.1 M sodium acetate, 0.1 M Bis-Tris, pH 6.0, EVAPORATION, temperature 285K