4F7G
Crystal structure of talin autoinhibition complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-01-04 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979150 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.665, 86.876, 113.629 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 69.020 - 2.050 |
R-factor | 0.21245 |
Rwork | 0.210 |
R-free | 0.24900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.579 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.020 | 2.100 |
High resolution limit [Å] | 2.050 | 2.050 |
Number of reflections | 20930 | |
Completeness [%] | 89.2 | 51.2 |
Redundancy | 8.8 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 289 | 18.5% (w/v) PEG 1500, 0.1 M MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |
2 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 289 | 18.5% (w/v) PEG 1500, 0.1 M MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |