4F4P

SYK in COMPLEX WITH LIGAND LASW836

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	CCD
Collection date	2008-07-25
Detector	MARRESEARCH
Wavelength(s)	1.000
Spacegroup name	P 21 21 21
Unit cell lengths	39.501, 84.227, 89.819
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.120 - 2.370
R-factor	0.2409
Rwork	0.238
R-free	0.28460
RMSD bond length	0.008
RMSD bond angle	1.045
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	38.120	2.570
High resolution limit [Å]	2.370	2.370
Rmerge	0.088	0.788
Number of reflections	12709
Completeness [%]	94.7	94.5
Redundancy	5.1	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1