4ELK
Crystal structure of the Hy19.3 type II NKT TCR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.220, 101.530, 134.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.233 - 2.100 |
R-factor | 0.1904 |
Rwork | 0.188 |
R-free | 0.22650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2q86 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.037 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.000 | 2.150 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.079 | 0.563 |
Number of reflections | 59222 | |
<I/σ(I)> | 11.5 | 2.5 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.1 | 295 | 18% PEG 4000, 0.2M ammonium citrate dibasic, pH 5.1, VAPOR DIFFUSION, SITTING DROP, temperature 295K |