4EKK
Akt1 with AMP-PNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-12-08 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.637, 55.853, 91.402 |
Unit cell angles | 90.00, 103.43, 90.00 |
Refinement procedure
Resolution | 29.690 - 2.800 |
R-factor | 0.2202 |
Rwork | 0.217 |
R-free | 0.27998 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.096 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.190 | 0.390 |
Number of reflections | 21128 | |
<I/σ(I)> | 5.7 | 2.4 |
Completeness [%] | 99.3 | 96.6 |
Redundancy | 3.4 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 293 | 20% PEG4K, 100mM Tris-pH7.5, Under Oil, temperature 293K |