4EDN
Crystal structure of beta-parvin CH2 domain in complex with paxillin LD1 motif
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 173 |
Detector technology | PIXEL |
Collection date | 2011-07-22 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.1 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 330.741, 55.842, 95.550 |
Unit cell angles | 90.00, 97.44, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.900 |
R-factor | 0.2301 |
Rwork | 0.228 |
R-free | 0.26510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.788 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Number of reflections | 38837 | |
<I/σ(I)> | 19.829 | 2.132 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.2 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | 2.1M Ammonium sulfate, 0.01M Tris, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |