4EAW
HCV NS5B in complex with IDX375
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-12-14 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.007 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 106.313, 108.028, 133.679 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.590 - 2.000 |
R-factor | 0.1732 |
Rwork | 0.173 |
R-free | 0.21863 |
Structure solution method | RIGID BODY |
RMSD bond length | 0.016 |
RMSD bond angle | 1.592 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.590 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 104093 | |
<I/σ(I)> | 2.48 | |
Completeness [%] | 99.7 | 99.7 |
Redundancy | 5.9 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |