4EAW
HCV NS5B in complex with IDX375
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-12-14 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 1.007 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 106.313, 108.028, 133.679 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.590 - 2.000 |
| R-factor | 0.1732 |
| Rwork | 0.173 |
| R-free | 0.21863 |
| Structure solution method | RIGID BODY |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.592 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | REFMAC |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.590 | 2.110 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 104093 | |
| <I/σ(I)> | 2.48 | |
| Completeness [%] | 99.7 | 99.7 |
| Redundancy | 5.9 | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
