Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX II BEAMLINE I911-5 |
| Synchrotron site | MAX II |
| Beamline | I911-5 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-05-08 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 0.908 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 160.350, 88.540, 136.760 |
| Unit cell angles | 90.00, 95.99, 90.00 |
Refinement procedure
| Resolution | 19.950 - 1.700 |
| R-factor | 0.2358 |
| Rwork | 0.235 |
| R-free | 0.29200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1rts |
| RMSD bond length | 0.022 |
| RMSD bond angle | 1.956 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER (1.3.3) |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 20.000 | 20.000 | 1.730 |
| High resolution limit [Å] | 1.700 | 4.600 | 1.700 |
| Rmerge | 0.063 | 0.047 | 0.993 |
| Number of reflections | 207806 | ||
| <I/σ(I)> | 16.9 | ||
| Completeness [%] | 99.9 | 99.5 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 278 | K/Na Tartrate, PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 278K |
