4DDI
Crystal structure of human OTUB1/UbcH5b~Ub/Ub
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97922 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 173.739, 106.225, 134.689 |
Unit cell angles | 90.00, 123.74, 90.00 |
Refinement procedure
Resolution | 49.469 - 3.802 |
R-factor | 0.2212 |
Rwork | 0.218 |
R-free | 0.27310 |
Structure solution method | MIR |
RMSD bond length | 0.004 |
RMSD bond angle | 1.028 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.470 | 4.020 |
High resolution limit [Å] | 3.796 | 3.796 |
Number of reflections | 19737 | |
Completeness [%] | 97.0 | 83.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 293 | 25% PEG1500, 0.1 M SPG, pH 8.0, VAPOR DIFFUSION, temperature 293K |