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4DBZ

Crystal Structure of V151L Actinorhodin Polyketide Ketoreductase with NADPH

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.2
Synchrotron siteALS
Beamline8.2.2
Temperature [K]100
Detector technologyCCD
Collection date2009-02-25
DetectorADSC QUANTUM 315
Wavelength(s)0.99980
Spacegroup nameP 32 2 1
Unit cell lengths102.934, 102.934, 121.844
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution47.419 - 2.643
R-factor0.1807
Rwork0.179
R-free0.21800
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.008
RMSD bond angle1.132
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCCP4
Refinement softwarePHENIX ((phenix.refine: 1.7_650))
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]2.640
Number of reflections21581
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP92980.1 M Tris-Cl, 1.8 M Na malonate, pH 9.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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