Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X13 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-12-16 |
| Detector | MARRESEARCH SX-165 |
| Spacegroup name | I 41 2 2 |
| Unit cell lengths | 68.065, 68.065, 178.909 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 63.620 - 1.760 |
| R-factor | 0.19123 |
| Rwork | 0.189 |
| R-free | 0.22507 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2trt |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.844 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 27.100 | 1.870 |
| High resolution limit [Å] | 1.760 | 1.760 |
| Rmerge | 0.100 | 1.010 |
| Number of reflections | 20998 | |
| <I/σ(I)> | 14.5 | 2.28 |
| Completeness [%] | 98.2 | 91.5 |
| Redundancy | 8.5 | 7.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | 13% PEG 6000, 2 M KCL, PH 8.0 |
