4D5G
Structure of recombinant CDH-H28AN484A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Collection date | 2012-02-14 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 122.835, 122.835, 143.011 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.630 - 2.000 |
| R-factor | 0.1362 |
| Rwork | 0.134 |
| R-free | 0.17860 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.847 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 46.510 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.160 |
| Number of reflections | 73954 |
| <I/σ(I)> | 10.3 |
| Completeness [%] | 99.5 |
| Redundancy | 6.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
