4D52
CRYSTAL STRUCTURE OF FUCOSE BINDING LECTIN FROM ASPERGILLUS FUMIGATUS (AFL) IN COMPLEX WITH L-GALACTOPYRANOSE.
Replaces: 4UQ7Replaces: 4AHBExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 80.030, 70.440, 117.800 |
Unit cell angles | 90.00, 108.34, 90.00 |
Refinement procedure
Resolution | 111.820 - 1.760 |
R-factor | 0.15493 |
Rwork | 0.154 |
R-free | 0.17780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4agi |
RMSD bond length | 0.010 |
RMSD bond angle | 1.455 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.440 | 1.850 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.080 | 0.390 |
Number of reflections | 121067 | |
<I/σ(I)> | 12 | 3.2 |
Completeness [%] | 97.1 | 96.1 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 200 MM CACL2, 25% PEG 4K AND 100 MM TRIS, PH 8.5 |