4D4P
Crystal Structure of the Kti11 Kti13 heterodimer Spacegroup P65
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-11-07 |
Detector | DECTRIS PILATUS 6M-F |
Spacegroup name | P 65 |
Unit cell lengths | 152.060, 152.060, 203.850 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 110.614 - 2.999 |
R-factor | 0.2092 |
Rwork | 0.208 |
R-free | 0.23370 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.559 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.080 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.010 | |
Number of reflections | 53195 | |
<I/σ(I)> | 17.05 | 1.23 |
Completeness [%] | 99.6 | 94.9 |
Redundancy | 11.39 | 11.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 100 MM TRIS PH 8.4, 2 M LI2SO4 |