4D2T
Structure of MELK in complex with inhibitors
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-09-22 |
Detector | RIGAKU SATURN |
Spacegroup name | P 1 |
Unit cell lengths | 66.526, 75.410, 79.736 |
Unit cell angles | 86.03, 69.05, 90.03 |
Refinement procedure
Resolution | 48.540 - 2.700 |
R-factor | 0.2732 |
Rwork | 0.270 |
R-free | 0.34000 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.110 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Refinement software | BUSTER (2.11.5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.500 |
High resolution limit [Å] | 2.700 |
Rmerge | 0.070 |
Number of reflections | 39601 |
<I/σ(I)> | 5.9 |
Completeness [%] | 93.1 |
Redundancy | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |