4CXT
BTB domain of KEAP1 in complex with CDDO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-05 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 42.687, 42.687, 271.028 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.170 - 2.660 |
R-factor | 0.2122 |
Rwork | 0.211 |
R-free | 0.24000 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.000 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | CCP4 |
Refinement software | BUSTER (2.11.5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.170 |
High resolution limit [Å] | 2.660 |
Rmerge | 0.130 |
Number of reflections | 4283 |
<I/σ(I)> | 14.5 |
Completeness [%] | 100.0 |
Redundancy | 17.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |