4CMN
Crystal structure of OCRL in complex with a phosphate ion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2011-05-15 |
Detector | ADSC CCD |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 146.766, 146.766, 146.766 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.922 - 3.130 |
R-factor | 0.2151 |
Rwork | 0.210 |
R-free | 0.26280 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3mtc |
RMSD bond length | 0.006 |
RMSD bond angle | 0.997 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 103.780 | 3.300 |
High resolution limit [Å] | 3.130 | 3.130 |
Rmerge | 0.060 | 0.790 |
Number of reflections | 10068 | |
<I/σ(I)> | 10.5 | 1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 40.5 | 42.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.2 M ZINC ACETATE, 0.1 M NA-CACODYLATE PH 6.5, 10% ISOPROPANOL |