4CL7
Crystal structure of VEGFR-1 domain 2 in presence of Cobalt
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-06 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 27.746, 41.711, 94.694 |
Unit cell angles | 87.05, 82.25, 73.03 |
Refinement procedure
Resolution | 19.469 - 2.000 |
R-factor | 0.1707 |
Rwork | 0.168 |
R-free | 0.23320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1flt |
RMSD bond length | 0.006 |
RMSD bond angle | 0.983 |
Data reduction software | XDS |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.470 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.070 | 0.330 |
Number of reflections | 26362 | |
<I/σ(I)> | 10.74 | 3.01 |
Completeness [%] | 97.1 | 96.6 |
Redundancy | 1.8 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | CRYSTAL WERE OBTAINED BY HANGING DROP METHOD FROM 1MM VEGFR1-D2, 5MM HEPES/NAOH PH7.0, 10MM COCL2, 100 MM BIS-TRIS/HCL PH6.5 15%(W/V) PEG3350. |