4CDK
Structure of ZNRF3-RSPO1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 |
Unit cell lengths | 51.700, 80.160, 82.980 |
Unit cell angles | 66.27, 81.36, 80.66 |
Refinement procedure
Resolution | 44.706 - 2.800 |
R-factor | 0.2192 |
Rwork | 0.218 |
R-free | 0.24640 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.209 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.630 | 75.630 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.090 | |
Number of reflections | 29157 | |
Completeness [%] | 95.4 | |
Redundancy | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2M SODIUM BROMIDE AND 20% W/V PEG 3350 |