4CB0
Crystal structure of CpxAHDC in complex with ATP (hexagonal form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 287 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 145.198, 145.198, 246.051 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.527 - 3.300 |
R-factor | 0.2039 |
Rwork | 0.203 |
R-free | 0.22890 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.013 |
RMSD bond angle | 1.897 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.210 | 3.560 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.080 | 0.810 |
Number of reflections | 23821 | |
<I/σ(I)> | 31.3 | 5.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 25.1 | 26.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |