4CB0
Crystal structure of CpxAHDC in complex with ATP (hexagonal form)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 287 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 145.198, 145.198, 246.051 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 47.527 - 3.300 |
| R-factor | 0.2039 |
| Rwork | 0.203 |
| R-free | 0.22890 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.897 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.210 | 3.560 |
| High resolution limit [Å] | 3.300 | 3.300 |
| Rmerge | 0.080 | 0.810 |
| Number of reflections | 23821 | |
| <I/σ(I)> | 31.3 | 5.3 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 25.1 | 26.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
