4C9U
Xenopus ZNRF3 ectodomain in complex with Xenopus RSPO2 Fu1-Fu2 crystal form II
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-12-02 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 2 2 21 |
Unit cell lengths | 57.555, 57.620, 208.915 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.500 - 3.000 |
R-factor | 0.23132 |
Rwork | 0.227 |
R-free | 0.30964 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.013 |
RMSD bond angle | 1.648 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 52.230 |
High resolution limit [Å] | 3.000 |
Rmerge | 0.140 |
Number of reflections | 13655 |
<I/σ(I)> | 7.2 |
Completeness [%] | 93.9 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |