4C9R
Xenopus ZNRF3 ectodomain in complex with Xenopus RSPO2 Fu1-Fu2 crystal form I
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-02-18 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 55.990, 81.229, 71.632 |
| Unit cell angles | 90.00, 113.00, 90.00 |
Refinement procedure
| Resolution | 65.940 - 2.100 |
| R-factor | 0.19 |
| Rwork | 0.188 |
| R-free | 0.24608 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.604 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 66.000 |
| High resolution limit [Å] | 2.100 |
| Rmerge | 0.120 |
| Number of reflections | 32344 |
| <I/σ(I)> | 17.1 |
| Completeness [%] | 93.7 |
| Redundancy | 17 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
