4C9E
Mouse ZNRF3 ectodomain in complex with Xenopus RSPO2 Fu1-Fu2 (Seleno Met) crystal form II
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-03-03 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 |
Unit cell lengths | 70.991, 71.279, 72.109 |
Unit cell angles | 69.29, 61.48, 84.31 |
Refinement procedure
Resolution | 35.370 - 3.000 |
R-factor | 0.24977 |
Rwork | 0.245 |
R-free | 0.33378 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.509 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 35.340 |
High resolution limit [Å] | 3.000 |
Rmerge | 0.070 |
Number of reflections | 22849 |
<I/σ(I)> | 6.4 |
Completeness [%] | 98.6 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |