4C8T
Xenopus ZNRF3 ectodomain crystal form I
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-05-04 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.212, 58.669, 52.730 |
| Unit cell angles | 90.00, 93.58, 90.00 |
Refinement procedure
| Resolution | 37.690 - 2.400 |
| R-factor | 0.21778 |
| Rwork | 0.215 |
| R-free | 0.26528 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.631 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 37.700 |
| High resolution limit [Å] | 2.400 |
| Rmerge | 0.070 |
| Number of reflections | 11752 |
| <I/σ(I)> | 8.7 |
| Completeness [%] | 99.2 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
